Introduction

Micro Gas Turbines (MGTs) for co-, tri- or polygeneration are becoming progressively more widespread because of their reliability, flexibility, compactness and very low NOx emissions (Sun et al., 2012). Despite the on-going energy transition and the short-term impact due to the lingering COVID-19 pandemic, the global production of MGTs (especially in Europe) shows a promising increasing trend for the next decade (Palmer, 2021). Although the electrical efficiency is generally lower than the one for similar size internal combustion engines (Ofualagba, 2012), the high total efficiency of MGTs, which can reach 80% thanks to the extraction of the high exhaust gases thermal content through a recuperator (Beith, 2011) is one of the main reason for their increasing adoption. Moreover, exhaust heat can be further extracted by means of a heat exchanger for the production of hot water.

However, if on one side recuperation is beneficial for the overall system efficiency, on the other side it reduces the ability to cool down the hot mechanical components, such as the combustion chamber, being the inlet air largely warmer than what it would be without recuperation. In MGTs, the air entering the combustion chamber is often above 650°C (Enagi et al., 2017). The lower cooling capability, in addition to the higher flame temperature due to warmer inlet gases, causes very high temperatures in the metal components of the combustion chamber, with peaks of 1,200 K in some cases (Cirigliano et al., 2020). Frequent starts and stops induce mechanical stresses at the boundary between materials due to their different thermal expansion, which, if taking place too fast, may cause local permanent plastic deformations. Moreover, long exposure at high temperatures in combustion chambers can promote creep, which can induce thermal fatigue and potential failure of these components. The accumulation of damage in combustion chambers can hence be divided into two categories: the plasticity taking place during transient states (maneuvers, starts and stops) and the viscoplastic-based damage (creep damage) at steady state operation.

It is then necessary to take into account the material degradation due to the progressively increasing viscoplastic deformation; this can be done by adding a scalar parameter to the mechanical model. Commercial Finite Element Methods (FEM) codes, like ANSYS, allow the user to write their custom mechanical model. In this work, the development of a Fortran-based subroutine integrated into ANSYS APDL is presented. On so doing, creep, damage, and material degradation can be modeled. In this work, Lemaitre-Chaboche creep damage model is adopted (Lemaitre and Chaboche, 1978). Secondary creep and isotropic hardening are modeled for the high-temperature resistant alloy Inconel 718. The material degradation is considered by coupling the Young’s modulus with the introduced damage.

The novelty of this paper consists in the determination of Norton coefficients for Inconel 718, which instead of being assumed constant, are temperature dependent and based on experimental data. It is shown that the creep model and subroutine based on these new coefficients correctly reproduces creep, stress relaxation and damage under typical MGT operating temperatures. This model constitutes the foundation of a life-assessment analysis for combustion chambers under creep damage.

Numerical methods

Creep modelling

Creep is described as a time-dependent deformation of a material subjected to high temperature and loads below its yield strength for an extended period of time. Temperature, stress, time and material properties influence the rate of creep deformation. The creep phenomena is mainly divided into three stages; i.e., primary I, secondary II, and tertiary III. The three stages correspond to strain rates that are decreasing, constant, and increasing, respectively. Figure 1 depicts a typical creep strain versus time curve. The stage I in the curve indicates the primary creep where the creep strain rate decreases to a minimum value, due the fact that the material is experiencing an increase in creep resistance, attributed to a reduction in the density of free dislocations. The stage II is known as steady-state creep or secondary creep. This regime is also termed as a state of balance between the rate of dislocation generation and rate of recovery, where the former contributes to hardening and the latter to softening of the test material (Abe, 2014). In the tertiary creep stage, the creep rate increases rapidly until failure. This stage describes a softening stage, where the cracks are formed and propagate along the grain boundaries (Betten, 2008). In addition, the microscopic voids accumulate within the material, resulting in a decrease in the effective cross-sectional area (i.e., Necking), which raises the effective stress.

Figure 1.

Typical creep strain vs. time curve showing the three stages of creep.

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In order to capture the damage caused by creep, the modified Lemaitre-Chaboche model (Chaboche and Rousselier, 1983; Lemaitre, 1985) is used in this study. The effective stress concept Lemaitre and Chaboche (1978) defines the creep damage Dcr starting from the effective section S~ and the effective uniaxial stress σ:

(1)
σ~=SS~σ=σ1Dcr

where Dcr represents the macroscopic effect of the mechanical degradation due to creep voids, and S~=SSvoids. Hence, strictly speaking, Dcr would be defined as Dcr=Svoids/S. Given the difficulty to obtain a reliable measure of Svoids during operation, it is more practical to describe the status of Dcr as the integral of its time evolution:

(2)
Dcr(t)=0tD˙cr(t)dt

Equivalent Von-Mises stress and equivalent strain are defined in terms of their stress and strain components:

(3)
σeq=(σ1σ2)2+(σ2σ3)2+(σ3σ1)22
(4)
ϵeq=23(ϵ1ϵ2)2+(ϵ2ϵ3)2+(ϵ3ϵ1)2.

The total equivalent strain ϵeq is given by the sum of elastic, plastic, thermal and creep equivalent strains:

(5)
ϵeq=ϵeqel+ϵeqpl+ϵeqth+ϵeqcr

Creep mechanisms can generally be grouped into two categories: diffusion creep and dislocation creep. Diffusion creep is dominant at lower stresses, and is caused by the movement of vacancies; dislocation creep is present at higher stresses and is caused by the movement of dislocations through the lattice. When a dislocation encounters an obstacle (for example another defect), the former can either climb it (at mid stresses) or glide through it (at high stresses). The creep mechanisms acting in a material can be identified for a range of stresses and temperatures in a deformation map, according to the methods described by Frost and Ashby (1982). A deformation map of Inconel 718 is not available to the authors, but similar Nickel-based superalloys, such as IN738LC Carey et al. (1990) or MAR-M-200 Cieśla et al. (2016), show the onset of dislocation creep at half of the melting point (about 600C) and at stresses above 50 MPa. The operative conditions at which MGT combustion chambers are operated (metal temperature and stresses due to thermal strains) lay above these values. Moreover, it has been shown in other studies that the validity of creep power laws, for example the Norton law, can be extended by accounting for temperature-dependent parameters Golan et al. (1996) and Alain (1998) or by introducing recovery processes associated to the dislocation structure Das et al. (2022). Barbosa et al. (1988) used physics-based four stress- and temperature-dependent parameters to describe creep curves. McLean et al. (1992) modelled creep curves of single crystal superalloys using eight temperature- and stress-dependent parameters. On so doing, power law can be used to describe the creep behavior over an extensive range of stress and temperature. For these reasons, this work aims to model dislocation creep only, and to adapt the Norton law material parameters to different temperatures.

The derivative of creep equivalent strain in time (primary and tertiary creep) can be described in the form of its dependency on equivalent stress, temperature and either creep strain or time, by means of a power law:

(6)
ϵ˙eqcr=C1σeqC2ϵeqcrC3eC4/T,orϵ˙eqcr=C1σeqC2tC3eC4/T

where T is the temperature and t is the time. For secondary creep, however, the strain rate is constant, hence, C3 = 0:

(7)
ϵ˙eqcr=C1σeqC2eC4/T

where C1, C2 and C4 are material constants whose values are determined using creep tests. Equation 7 is the most important and widely used formulation to predict the secondary creep and is known as Norton power law. Table 1 shows the values of C1, C2 and C4 for Inconel 718 according to (Liu et al., 2015) and based on creep test data (Li et al., 2010). Note that for these parameters, stress is expressed in MPa, temperature in K, and strain in units per hour.

Table 1.

Norton coefficients for Inconel 718 according to (Liu et al., 2015).

C1C2C4
2.147·10−710.17150,825.89

The creep damage evolution is given by:

(8)
D˙cr=(σeqA)r(1Dcr)k

where Dcr is the scalar creep damage parameter. D˙cr is expressed in units per second and k is given by:

(9)
k=a0+a1(σeqz)+a2(σeqz)2

where a0, a1, a2, z, r and A are material constants which are determined again by creep tests. For Inconel 718 these values are reported in Table 2 (Zhang, 1995).

Table 2.

Material constants for damage evolution equation.

a0a1a2rZA
13.24780.7865·10−40.1924·10−313.19733.251,209

The scalar creep damage variable Dcr is zero for undamaged material and increases in time with Equation 8 up to an arbitrary value, usually 1, at which the material is assumed to fail. Basing on the damage theory of (Kachanov, 1999) and taking into account the concept of effective stress (Rabotnov et al., 1970) and the principle of strain equivalence (Lemaitre and Chaboche, 1978), changes in mechanical behavior can be measured through the evolution of the elastic modulus Lemaitre (1985):

(10)
E=E0(1Dcr)

where E is the effective elastic modulus and E0 is the Young’s modulus of undamaged material. By differentiating Equation 10 in time, one obtains:

(11)
E˙=E0D˙cr=E0(σeqA)r(1Dcr)k

By remembering the constitutive relation between σ, ϵel and the elasticity matrix [D], which contains E (Chandrupatla and Belegundu, 2012), one can derive:

(12)
σ˙=[D].ϵel+[D]ϵ˙el

Equation 12, together with Equations 7 and 8, constitute a system of nonlinear differential equations in σeq, Dcr and ϵeqcr, where T can be constant or vary with time too. Also by remembering the fact that ϵeqel and ϵeqcr are related by Equation 5, it is clear how this highly coupled problem needs to be solved by a dedicated code.

Material parameters identification

In applying the Norton formulation (Equation 7) to the analysis of structures one should bear in mind that the material parameters C1, C2 and C4 are obtained by interpolating experimental creep tests, hence their validity is limited to the narrow range of stresses and temperatures the tests were conducted. In the previous section, a set of these parameters is proposed in Table 1. However, the use of only three constants to cover the whole spectrum of stresses and temperatures a structure can be subjected to might introduce relevant inaccuracies in the model. For this reason, in this paper a whole new set of parameters was derived from the creep tests of Inconel 718 at different temperatures performed by (Brinkman et al., 1991). In Figure 2, the results of the creep tests are shown. In this section, a method to derive Norton parameters from creep tests is highlighted.

Figure 2.

Creep-rupture lifetime data and numerical interpolation for Inconel 718.

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Since the secondary creep stage is characterized by a constant creep strain rate, one can assume dϵeqcr/dtϵeq,sscr/tss, where ϵeq,sscr and tss are the equivalent creep strain and the time to the onset of tertiary creep, respectively. Hence, the Norton relation (Equation 7) can be rewritten in the form:

(13)
σeq=(ϵeq,sscrexp(C4/T)C1tss)1/C2

where T, tss and σeq are expressed in Kelvin, hours and MPa respectively. The time to the onset of tertiary creep can be related to the time to rupture for Inconel 718 by (Brinkman et al., 1991):

(14)
tss=Atrβ

with A = 0,442 and β = 1,04 up to tr=105h, and A = 0,7 and β = 1 above. Relating ϵeq,sscr with the creep strain to rupture, ϵeq,rcr, remains an harder task, due to the large amount of scatter which is typical in creep measurements. For temperatures between 650C and 760C, some creep tests indicate ϵeq,rcr between 3% and 9%, increasing with temperature (Kim et al., 2008; Sugahara et al., 2012; Caliari et al., 2016). A more handy correlation is given again by (Brinkman et al., 1991):

(15)
ϵeq,sscr=0.2+ABtr(βα)

where A and β are the same as shown above, 0.2 is the elastic strain offset, and B and α are reported in Table 3.

Table 3.

B and α parameters.

tr(h)T(C)Bα
<11,000≥5932.1421.151
<11,000≤59334.1821.443
≥11,000Any2.1421.151

In this way, the determination of temperature-dependent parameters C1, C2 and C4 can finally take place as follows:

  1. Obtain from creep tests points (σ,tr) at different temperatures;

  2. compute tss from Equation 14 with the corresponding A, β;

  3. compute ϵeq,sscr from Equation 15 with the corresponding B,α;

  4. substitute tss and ϵeq,sscr in Equation 13;

  5. for every temperature T, find the values {C1, C2, C4} giving a σeq as close as possible to the one of the tests (point 1).

The key point of this approach is noting that creep tests are performed at constant stress, hence, one can use the same σeq of the creep rupture tests to relate the tr to the state on onset of tertiary creep, tss and ϵeq,sseq of Norton formulation, which is generally not known. The new set of parameters for Inconel 718 is presented in Table 4. By applying these parameters in Equation 13, interpolating curves are generated and plotted in Figure 2, showing excellent fit. A comparison between the use of constant parameters and temperature-dependent parameters can be well appreciated in a 3D space (Figure 3).

Table 4.

Norton equation coefficients at different temperatures for Inconel 718.

T (°C)C1C2C4
4271.10·10−921.8109,000
4823.00·10−915.884,000
5384.00·10−914.481,000
5932.00·10−912.371,000
6491.00·10−75.434,500
7045.00·10−63.729,000
7602.00·10−74.528,000
Figure 3.

Creep-tests can be plotted in a three-dimensional space, where each point is represents a test conducted at a specific σeq, tr and T. By computing the creep strain with the Norton law, a 3D surface can be obtained and overlapped to experimental data. A comparison between constant parameters (a) and temperature-dependent parameters (b) shows a much better fit of the latter. (a) Constant coefficients (Table 1). (b) Variable coefficients (Table 4).

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User programmable feature USERMAT in ANSYS

In this section, the implementation of a damage-based material model in the commercial software ANSYS APDL is outlined. User Programmable Features (UPFs) are a highly effective and flexible tool to tailor the behavior of the APDL program to suit individual requirements. This is performed by writing a custom subroutine in the C, C++, or Fortran programming languages. One of such subroutines is USERMAT, which is particularly used to define non-linear stress-strain relationships of elastic-plastic materials, custom damage evolution and creep laws, like in this study.

USERMAT subroutine is called at every iteration and executed on each element of the computational grid. The input parameters, such as loads and temperature, are defined by the user during the modelling step. Current stresses, strains and strain increments are the inputs at the start of the timestep. At each iteration, a new elastic, plastic, thermal and creep strain, an effective Young’s modulus and damage evolution are computed based on the constitutive equations and material model described in the previous sections. USERMAT then updates the stresses and the material Jacobian matrix and these values are sent back to the main Finite Element code as outputs (Lin, 1999). The status of every element is checked at every time increment using a strength lifetime failure criterion: when the maximum damage of the structure reaches a threshold value, the subroutine is stopped and the present time is recorded as the lifetime of the component. In this analysis, Dcr=0.4 is considered as the the maximum allowable damage.

The geometry chosen is a rectangular bar of Inconel 718 alloy with a base of 10 × 10 mm and a length of 100 mm. The bar is discretized with 2 hexahedral elements for each short side and with 20 along the length (80 elements in total). Since the application of the present work is three-dimensional and plain strain, SOLID186 elements (20 nodes each, second-order shape functions) are used. The bar is fixed at one end and a displacement is applied to the opposite end to obtain the uni-axial stress state. Material properties of Inconel 718 such as density, thermal expansion coefficients and Young’s modulus (of undamaged material) are taken from data sheets (VDM Metals, 2020).

Results and discussion

The application of the described UPF using the temperature-dependent coefficients is presented in this section. Temperature is set to 750 K. The comparison between the experimental tests, the Norton-Damage model with constant parameters of (Liu et al., 2015) and the Norton-Damage model of this analysis is depicted in Figure 4.

Figure 4.

Comparison between experimental data, the use of the constant parameters from (Liu et al., 2015) and the new, temperature-dependent parameters, at 750 K and initial σ = 700 Mpa.

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In the experiments, a displacement is applied to one end in order to generate an initial stress of 700 MPa; shortly after, the stress relaxes to a much lower value, around 635 MPa, showing the typical primary creep phase. Afterwards, the stress stabilizes and slowly decreases, due to further stress relaxation. Finally, a rapid decrease in the cross-sectional area of the probe brings the material to failure.

For the two simulations, since the Norton equation only models the secondary creep, an initial σ=635MPa is set. The decrease of equivalent stress is due to a decrease in effective Young’s modulus, in turn due to damage accumulation, as expected (see Equation 10). Both the stress decrease and the damage increase are represented with good accuracy when compared to the experimental data, except from the areas at the very beginning and at the end of the simulations, where the stress decreases relatively fast. Those are the areas corresponding to primary and tertiary creep. It must be remembered that this UPF is developed to model secondary creep, hence, the high strain rates typical of primary and tertiary creep are out of the scope of this paper.

The temperature-dependent parameters allow the user to span over a wider range of (in particular to higher) temperatures, compared to those parameters of (Liu et al., 2015), which are optimized for 750 K only. As an example, creep strain and damage over time at three different temperatures and for an initial stress of 650 MPa are shown in Figure 5. It can be seen that temperature has an enormous impact on creep and on creep strain, as expected. Higher temperatures promote a much faster creep deformation. This is depicted well from the picture on the right. On the left, the damage shows again a non-linear increasing trend with time. Since the Chaboche-Lemaitre damage Dcr depends on equivalent stress only (at least directly, see Equations 8 and 9), the damage evolution is, in the first phase, very similar for all the temperatures. Over time, the damage increases more at higher temperatures, both due to higher creep and lower Young’s modulus with temperature.

Figure 5.

Damage and creep strain at three different temperatures and initial σ = 650 Mpa.

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Conclusions

In this paper, a method for the determination of temperature-dependent Norton coefficients for Inconel 718 was shown. The procedure takes rupture creep test data as input. The so obtained coefficients are then implemented in a User Programmable Feature inside the ANSYS APDL environment, enabling the user to write a custom mechanical model. In this study, secondary creep together with material damage and Young’s modulus reduction were combined.

The results show excellent agreement with the experimental data, strictly concerning the secondary creep portion of the tests. The UPF allows the simulation of creep damage in a wide range of temperatures, in particular up to 760°C, which are close to the temperatures typical of a gas turbine combustion chamber. This method has the potential to be extended to even higher temperatures, if creep tests are provided. The range 760–1,000°C is currently under development.

This study constitutes the foundation to explore the life of Inconel 718 structures exposed at high temperature creep, where stress relaxation, damage and creep are taken into account for a realistic representation of this coupled problem. The direct application of this USERMAT subroutine in ANSYS to MGT combustion chambers is currently under development and will be published on basis of a separate study.

Nomenclature

Latin symbols

[D]

elasticity matrix

Dcr

creep damage

E

effective Young’s modulus

E0

undamaged Young’s modulus

MGT

Micro Gas Turbine

tr

rupture time

tss

time at III creep onset

UPF

User Programmable Feature

Greek symbols

ϵ

strain tensor

ϵeq

equivalent total strain

ϵeqcr

equivalent creep strain

ϵeq,sscr

eq. creep strain at III creep onset

ϵeqel

equivalent elastic strain

ϵeqpl

equivalent plastic strain

ϵeqth

equivalent thermal strain

σ

stress tensor

σeq

equivalent stress